Journal :   Asian Journal of Research in Chemistry

Volume No. :   4

Issue No. :  8

Year :  2011

Pages :   1243-1244

ISSN Print :  0974-4169

ISSN Online :  0974-4150


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Microwave Induced Synthesis of Azo Compound: A Solvent Free Path For Some Dyes



Address:   Nirupma Jadon and Sadhana Singh*
Department of Chemistry, B.N.P.G. College, Udaipur (Raj.) India – 313001
*Corresponding Author
DOI No:

ABSTRACT:
An efficient method for the exclusive one pot synthesis of sodium salt of Benzidine diazo-bis-1-naphthyl amine-4-sulphonic acid (An Azo compound) under conditions of microwave irradiation. The Reaction was found to follow diazotization and condensation mechanism with removal of water molecules. Formation of product was confirmed through TLC, M.P. and spectral analysis. The reaction was carried out in a single pot without using solvent in a domestic microwave oven and Sodium 4-[{4-[(2-nitrophenyl)amino]phenyl}diazenyl] benzene sulfonate.
KEYWORDS:
Sodium salt of Benzidine diazo-bis-1-naphthyl amine-4-sulphonic acid (An Azo compound), microwave irradiations, one pot synthesis, dyes, solvent free path, IR and Mass Spectroscopy and Sodium 4-[{4-[(2-nitrophenyl)amino]phenyl}diazenyl] benzene sulfonate.
Cite:
Nirupma Jadon, Sadhana Singh. Microwave Induced Synthesis of Azo Compound: A Solvent Free Path For Some Dyes. Asian J. Research Chem. 4(8): August, 2011; Page 1243-1244.
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