Journal :   Asian Journal of Research in Chemistry

Volume No. :   5

Issue No. :  9

Year :  2012

Pages :   1172-1175

ISSN Print :  0974-4169

ISSN Online :  0974-4150


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Synthesis and Characterization of Novel Oxadiazole Derivatives of 2-mercaptobenzothiazol– A Green Approach



Address:   Sushil R.M., Rohikar R.V., Hanumant G.G., Akuskar S.K., Amit N.V.*
P.G. Research Center, Department of Chemistry, S.M.P. College, Murum -413605 Maharashtra, India.
Corresponding Author
DOI No:

ABSTRACT:
Novel 2-Mercaptobenzothiazole derivatives synthesized from 2- Mercaptobenzothiazole reacted with ethyl chloroacetate to get ester derivatives (3) using Green method. These ester converted to hydrazids (4) by reaction with hydrazine hydrate under MWI. 5-substituted 1,3,4-oxadiazole (5a-g) synthesized from hydrazide, substituted benzoic acid and phosphprous oxochloried by Microwave irradiation as reported in literature. The structure of newly synthesized compound was established by physico-chemical and spectral data analysis.
KEYWORDS:
2-Mercaptobenzothiazole, hydrazine hydrate, substituted1,3,4-oxadiazole, substituted benzoic acid, Microwave irradiation.
Cite:
Sushil R.M., Rohikar R.V., Hanumant G.G., Akuskar S.K., Amit N.V.. Synthesis and Characterization of Novel Oxadiazole Derivatives of 2-mercaptobenzothiazol– A Green Approach. Asian J. Research Chem. 5(9): September, 2012; Page 1172-1175.
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