Journal :   Asian Journal of Research in Chemistry

Volume No. :   7

Issue No. :  8

Year :  2014

Pages :   702-710

ISSN Print :  0974-4169

ISSN Online :  0974-4150


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Synthesis, Characterization and Study of Chromatography Behavior of Novel (Azo–Anil)-Heterocyclic Compounds



Address:   Dr. Nagham Mahmood Aljamali1*, Dr. Khdeeja Jabbar Ali1, Nuha Salman Salih2, Dr. Sajida Hadi Ridha1
1Assist .Professor, Dept. of Chem., Educt. College, Kufa Univ., Iraq
2Lecturer, Dept of Chem., Science College, Kufa Univ., Iraq
*Corresponding Author
DOI No:

ABSTRACT:
The present work included synthesis of novel (azo-anil) compounds in high yield, which react with (chloro acetyl chloride, sodium azide, alanine, o-thiol via condensation reaction to produce various heterocycles (four, five, six, seven) membered ring like (azetidine, imidazole, thiazine, oxazepine, diazepine, tetrazole) The structure of the newly synthesized compounds were monitored by (TLC) and identified by many techniques (FT.IR, 1H.NMR, C.H.N), melting points and study of chromatography behavior .
KEYWORDS:
Chromatography, azo–anil, heterocycle, thiazine, diazepine.
Cite:
Nagham Mahmood Aljamali, Khdeeja Jabbar Ali, Nuha Salman Salih, Sajida Hadi Ridha. Synthesis, Characterization and Study of Chromatography Behavior of Novel (Azo–Anil)-Heterocyclic Compounds. Asian J. Research Chem. 7(8): August 2014; Page 702-710.
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