ISSN

0974-4150 (Online)
0974-4169 (Print)


Author(s): Veena Yadav, Nishant Yadav

Email(s): veenayadav2006@gmail.com

DOI: Not Available

Address: Veena Yadav* and Nishant Yadav
Department of Chemistry, Kurukshetra University, Kurukshetra (India)
*Corresponding Author

Published In:   Volume - 4,      Issue - 4,     Year - 2011


ABSTRACT:
An efficient microwave assisted protocol for the synthesis of Mannich’s bases of isatoic-anhydride derivatives 4(a-g) has been described. Treatment of isatoic anhydride (1) with formaldehyde yielded 1-hydroxymethyl-1H-benzo[d][1,3]oxazine-2,4-dione (2) followed by reaction with HCl afforded 1-chloromethyl-1H-benzo[d][1,3]oxazine-2,4dione (3) which reacted smoothly with sec. amines to give mannich’s bases 4(a-g) in excellent yield.


Cite this article:
Veena Yadav, Nishant Yadav. Microwave Assisted Facile Synthesis of Some Novel Mannich’s Bases of Isatoic Anhydide Derivatives. Asian J. Research Chem. 4(4): April, 2011; Page 626-628.


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